Simultaneous Thermogravimetric Analysis
Simultaneous Thermogravimetric Analysis
Make
Hitachi
Model
NEXTA STA300
Facility Status
Working
Facility Management Division
Sophisticated Analytical Instrument Facility (SAIF)

Category

  • Material Characterization » Thermal Characterisation

Booking Details

Booking available for
Internal and External Both
Available Mode for Use
Temperature Range : RT to 1500 ℃ Regular use : RT to 1300 ℃ Scanning Rates : 0.1 to 100 ℃ DTA Measurement range : ± 1000 µV Gas Type : N2, Air, Ar, O2 Gas Flow rates : 50 to 500 ml/min Auto sampler : 50 samples

Facility Management Team and Location

Faculty In Charge
Prof. Suparna Mukherji, Head, SAIF & CRNTS
office.saif@iitb.ac.in
022- 2576-7691
Facility Manager
Dr. Nutan Agadi
nmagadi@iitb.ac.in
022- 2159-6889
Department
CRNTS
LAB Email ID
nmr600@iitb.ac.in
Lab Phone No
022-2159 6866/89

Facility Features, Working Principle and Specifications

Features Working Principle

Simultaneous Thermogravimetric Analysis is a method in which thermogravimetry and differential thermal analysis are combined and measured simultaneously by a single apparatus.

Thermogravimetry (TGA) is a technique that measures mass change in a sample as a function of time and temperature, and it is used to detect evaporation, decomposition, oxidation and other effects of temperature change that cause mass changes. 

Differential Thermal Analysis (DTA) measures the temperature difference between a sample and a reference as the temperature is increased. Changes in the sample, either exothermic or endothermic, can be detected relative to the inert reference. Thus, a DTA curve provides data on the transformations that have occurred, such as glass transitions, crystallization, melting and sublimation.

Instructions for Registration, Sample Preparation, User Instructions, Precautionary Measures and Charges

User Instructions and Precautionary Measures

Charges (including 18% GST) *For Thermal Analysis, standard ramp is 10 ℃/min. Heating rates less than standard rate will be charged by hours:

 AcademicNational LabIndustryIIT Bombay
 Heating Program: Temp. Range @ 10 ℃/minRs.Rs.Rs.Rs.
    
 RT - 600 ℃  944  2832  4720  400
 RT - 800 ℃  1180  3540  5900  500
 RT - 1000 ℃  1534  4602  7670  650
 RT - 1200 ℃  1888  5664  9440  800
 RT - 1450 ℃  2360  7080  11800  1000

 


 

Applications

Changes in mass due to decomposition, oxidation, evaporation, or combustion.

Volatilization rate of materials, Moisture content & Solvent content.

Thermal Stability for quality assurance and safety purposes.

Kinetics analysis.

Additives, Polymer content, Filler content, etc.

Glass transitions, Endothermic(Melting) and Exothermic reactions (Crystallization)

Sample Details

SOP, Lab Policies and Other Details

Publications

Publications
NA