Laser Raman Spectrometer Facillity
Laser Raman Spectrometer Facillity
Make
Horiba Jobin Yovon, France
Model
Labram HR800 UV
Facility Status
Working
Facility Management Division
Institute Central Research Facilities (ICRF)

Category

  • Spectroscopy and Spectrometry » Raman Spectrometer

Booking Details

Booking available for
Internal and External Both
Available Mode for Use
Confocal Laser Raman spectrometer

Facility Management Team and Location

Faculty In Charge
Prof. Sagar Mitra
Co-convenors
Prof. A. R. Bhattacharyya
Prof. Leela S. Panchakarla
LAB Email ID
lrs@iitb.ac.in
Facility Location
Room No.: 208A, First floor, Centre for Center for Research in Nano Technology and Science building.
Lab Phone No
022-2576-7654

Facility Features, Working Principle and Specifications

Features Working Principle
  • Imaging/Mapping:

XYZ mapping:

XY stage :X=75 mm and Y=50 mm , 1 µm repeatability

Step-by-step mode: step size (min) 50 nm

Z stage min step = 0.1 µm 

Duoscan Mode with scanning mirror.

Scanning/Averaging followed by Macro mapping for large area mapping

  • Polarization dependent Raman Scattering :Range 400 – 700 nm
  • Low Temp : Min 80K

Raman scattering is an inelastic scattering of incident light from vibrating atoms or molecules or from electronic states like plasmons, coupled plasmon-phonon states etc with change in the wavelength. It consists of Stokes and anti-Stokes components depending on whether the scattered wavelength is greater or less than the incident one. Thus Raman spectrum from a sample consists of several lines characteristic of the unique vibrational modes of the sample and has turned out to a fast and reliable non-destructive technique for characterization, material property studies under different sample environment.  However the Raman scattering efficiency is very poor and ≈ 10-3 – 10-5 times the elastically scattered Rayleigh component and requires a powerful excitation source. The excitation sources are generally UV/VIS/NIR CW laser sources with high incident photon flux and detection is by highly efficient CCDs. The change in the wavelength of the scattered radiation is analyzed using a single/multiple grating high resolution UV-visible-NIR optical spectrometer/spectrograph. The spectrometer should possess a very high rejection capability of the elastically scattered Rayleigh component from much weaker Raman scattered light. This is usually achieved by two or three stage spectrometers or more recently by single stage spectrometers with highly efficient Holographic Notch filters or sharp cutoff dielectric edge filters. 

Instructions for Registration, Sample Preparation, User Instructions, Precautionary Measures and Charges

Instruction for Sample Preparation
  • Samples can be solid in form of powder, thin film or bulk pallets. Solid samples should preferably not exceed size of 50 mm X 50 mm X 20 mm and not weigh more than 100 gms.
  • Sample should be nontoxic and non radiactive.
  • Liquid samples will be done in thin walled (< 0.5 mm and 2 mm OD ) glass/quartz capillary tubes. Users are required to bring samples in sealedcondition.

 

User Instructions and Precautionary Measures
  • Only online registration will be accepted. If you need to cancel your slot, send an email immediately to with an explanation. Else user will be blocked after two repeat ‘no show’
  • Slots will be provided on a first-come first-served basis as far as possible.
  • The slots are from 10.30–12.00, 12.00 – 13.30, 14.30- 16.00, 16.00 – 17.30 hrs. You can request two consecutive slots only once in a week. If your experiment needs more time (e.g. Mapping/Imaging.), please indicate area, mapping step, scan range (cm-1) and integration time so that we can deal with your specific requirement.
  • USB drives are strictly forbidden for copying data to minimize virus-related issues. You need to bring a new blank CD to transfer your data. All data must be transferred within 7 days without exception.
  • Users must be available throughout the course of data acquisition.

Applications

Sample Details

SOP, Lab Policies and Other Details

Publications

Publications
NA