CHNSO Elemental Analyzer

External users: registration to be carried out only through I-STEM portal
Additional information about sample and analysis details should be filled in the pdf form provided in the I-STEM portal under “DOWNLOAD CSRF”

Internal users (IITB): registration to be carried out only through DRONA portal
Additional information about sample and analysis details should be filled in the pdf form provided here.

CHN_MSDS (1)_0.pdf (322.76 KB)
Make
ThermoFisher Scientific
Model
Flash smart V CHNS/O
Facility Status
Working
Date of Installation
Facility Management Division
Sophisticated Analytical Instrument Facility (SAIF)

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Category

  • Material Characterization » Chemical Characterisation

Booking Details

Booking available for
Internal and External Both

Facility Management Team and Location

Facility In Charge
Head SAIF
Facility Manager
Dr. Bharati Patro, bharati@iitb.ac.in
Facility Operator
Ms. Mursaleen Shaikh, mursaleen@iitb.ac.in
Ms. Pallavi Khapre, pallaviag@iitb.ac.in
Department
Sophisticated Analytical Instrument Facility (SAIF)
Lab Email ID
mursaleen@iitb.ac.in, pallaviag@iitb.ac.in
Facility Location
112-B, Ground Floor, SAIF
Lab Phone No
022-2159 6884/ 6376

Facility Features, Working Principle and Specifications

Features Working Principle

The CHNS(O) Analyzer find utility in determining the percentages of Carbon, Hydrogen, Nitrogen, Sulphur and Oxygen of organic compounds, based on the principle of "Dumas method" which involves the complete and instantaneous oxidation of the sample by "flash combustion". The combustion products are separated by a chromatographic column and detected by the thermal conductivity detector (T.C.D.), which gives an output signal proportional to the concentration of the individual components of the mixture.

There are different techniques for the determination of CHN\CHNS\O. It brings a new level of precision, accuracy, speed of analysis and ease of operation.The built in chromatographic column converts the compound and elutes it in the form of NO2,CO2, SO2,H2O which are then detected with the help of Thermal Conductivity Detector.

The instrument is calibrated with the analysis of std compounds using the K-factors calculations. Thus the instrument ensures maximum reliability of the results because the combustion gases are not split or diluted but directly carried to build in GC system simultaneous determination of CHNS can be done in less than 10 mins. This method finds greatest utility in finding out percentages of C, H, N, S, (O) in organic compounds which are generally combustible at 1800o C.

Key components of CHNS are auto sampler, combustion reactors ,chromatographic column, and T.C.D. detector.

Sample Preparation, User Instructions and Precautionary Measures

User Instructions and Precautionary Measures
  1. Sample must be pure and all contaminants must be removed.

  2.  Sample weight should be in between 4-5 mg.

  3.  Liquid samples should have constant weight

CHNS (O) Analyzer Charges:

Sr. No.

Category

CHNS  

Oxygen  

GST@ 18%

1.

IITB  Students

300

300

-

2.

IITB-Monash Students

300

300

18% GST

3.

Academic Institutes

600

600

18% GST

4.

National Labs

1500

1500

18% GST

5.

SINE (letter from SINE reqd.)

1500

1500

18% GST

6.

Research Park (MSME) (letter from RP reqd.)

1500

1500

18% GST

7.

Research Park 

(Big Industry partners)

(letter from RP reqd.)and MSME not associated with RP (appropriate certificate required)

2250

2250

18% GST

8.

Industries

3000

3000

18% GST

 

Charges for Analytical Services in Different Categories

Applications

  • Organic compounds
  • Pharmaceuticals
  • Food & Agricultural Industries
  • Chemistry & Chemical Engineering
  •  Geological & Environmental samples
  •  Organometallics
  •  Gasoline and fuels
  •  Coal and coke
  •  Graphite and carbides
  •   Metals and alloys
  •   Polymers and explosives
  •   Building materials and your samples…

Sample Details

SOP, Lab Policies and Other Details

Publications