ATR-FTIR
Make
Bruker
Model
Alpha II
Facility Status
Working
Date of Installation
Facility Management Division
Centre for Sophisticated Research Facilities (CSIF- IoE Funded*)

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Category

  • Spectroscopy and Spectrometry ยป Optical Spectroscopy

Booking Details

Booking available for
Internal and External Both
Available Equipment/ Mode of use
ATR mode
Transmission mode for both solids and liquids

Facility Management Team and Location

Faculty In Charge
Prof. Kamendra P. Sharma
Facility Manager
Mr. Amol Hanumante
Facility Operator
Mr. Amol Hanumante
Facility Management Members
Prof. Kamendra P. Sharma
Prof. Nandita Madhavan
Prof. Ajay S. Panwar
Prof Shobhna Kapoor
Department
Chemistry
Lab Email ID
amol_ah@iitb.ac.in
Facility Location
Room No 360, Chemistry Department Facility lab II, 2nd floor, Chemistry Building, IIT Bombay
Lab Phone No
022-25764159

Facility Features, Working Principle and Specifications

Facility Description

Facility Description

Alpha II is very compact ATR-FTIR spectrometer for quick, easy and reliable IR analysis.

Features Working Principle

Features/ Accessories: 

  • Diamond ATR
  • Spectral Range: 4000-500 cm-1
  • Rock Solid Cube Corner Interferometer
  • Detector: Temperature controlled DLATGS detector
  • Spectral range : 2 cm-1 or better 
  • Optics: ZnSe Beamsplitter and ZnSe windows
  • Demountable transmission cells with circular CaF2 windows

Principle:

An attenuated total reflection accessory operates by measuring the changes that occur in a totally internally reflected infrared beam when the beam comes into contact with a sample. An infrared beam is directed onto an crystal with a high refractive index at a certain angle. This internal reflectance creates an evanescent wave that extends beyond the surface of the crystal into the sample held in contact with the crystal. The sample absorbs IR energy. The attenuated energy from each evanescent wave is passed back to the IR beam, which then exits the opposite end of the crystal and is passed to the detector in the IR spectrometer which generates an infrared spectrum.

Instructions for Registration, Sample Preparation, User Instructions and Precautionary Measures

Instructions for Registration

User must contact the Technical operator before booking slot and discuss the experimental parameter like Scanning Range, Number of Scan, Nature of Sample etc

 

Instruction for Sample Preparation
  • If Any reference material, is to be supplied by the user
  • Provide solid samples in the fine powder form. 
  • In case any additional Chemicals/ materials  required for recording the samples, Charges would be additional.
User Instructions and Precautionary Measures

MS-DS (Material Safety Data Sheet) should be given along with samples. Samples should not be toxic or hazardous. 

Charges for Analytical Services in Different Categories

Usage Charges

 

Type of analysis

 

IITB users

Academic institutes

National

R&D lab

Industries / Non-Govt. Agencies

Sample Charges

 

100

200

500

1000

                                      All charges in INR. For external samples, in addition to above basic charges prevailing GST will be added.

Applications

Sample Details

Chemical allowed

Yes

Allowed Substrate

No

Gases allowed

No

Substrate Dimension

No

Target dimension

No

Contamination remarks

No

Precursors/ Targets allowed

No

SOP, Lab Policies and Other Details

Publications

na